6H09
HIV capsid hexamer with IP6 ligand
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-03-03 |
Detector | OXFORD RUBY CCD |
Wavelength(s) | 0.987 |
Spacegroup name | P 6 |
Unit cell lengths | 91.099, 91.099, 57.111 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.300 - 2.000 |
R-factor | 0.23914 |
Rwork | 0.238 |
R-free | 0.26620 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.551 |
Data reduction software | iMOSFLM |
Data scaling software | pointless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0230) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 78.900 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmeas | 0.898 | |
Number of reflections | 18396 | |
<I/σ(I)> | 2 | 2.4 |
Completeness [%] | 99.7 | 96.5 |
Redundancy | 4.9 | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 293 | PEG 4K |