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6GZW

Ferric DtpA from Streptomyces lividans

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE MASSIF-3
Synchrotron siteESRF
BeamlineMASSIF-3
Temperature [K]100
Detector technologyPIXEL
Collection date2016-12-15
DetectorDECTRIS EIGER X 16M
Wavelength(s)0.9677
Spacegroup nameP 1 21 1
Unit cell lengths60.118, 71.032, 78.089
Unit cell angles90.00, 92.83, 90.00
Refinement procedure
Resolution77.990 - 1.410
R-factor0.1905
Rwork0.189
R-free0.21630
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)5map
RMSD bond length0.011
RMSD bond angle1.513
Data reduction softwareEDNA
Data scaling softwareAimless (0.5.29)
Refinement softwareREFMAC
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]77.9901.460
High resolution limit [Å]1.4101.410
Rmerge0.1271.253
Rmeas0.1411.391
Rpim0.0600.593
Number of reflections1183399905
<I/σ(I)>7.8
Completeness [%]93.980.4
Redundancy5.25.1
CC(1/2)0.9970.529
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP5.5291Crystals were grown by the vapour diffusion hanging drop method using a ferric protein solution at 13 mg/ml equilibrated against a reservoir consisting of 17-24% PEG 3000 and 50-100 mM sodium citrate, pH 5.5.

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