6GY4
Crystal structure of the N-terminal KH domain of human BICC1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-09-30 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9212 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 44.406, 153.164, 86.235 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.740 - 1.986 |
R-factor | 0.2579 |
Rwork | 0.256 |
R-free | 0.30350 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1zzk |
RMSD bond length | 0.003 |
RMSD bond angle | 0.514 |
Data reduction software | XDS |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.740 | 2.164 |
High resolution limit [Å] | 1.986 | 1.986 |
Rmerge | 0.099 | 0.949 |
Rpim | 0.043 | 0.457 |
Number of reflections | 11724 | 576 |
<I/σ(I)> | 10 | 1.6 |
Completeness [%] | 90.5 | 67.5 |
Redundancy | 6.4 | 5.2 |
CC(1/2) | 0.999 | 0.682 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.1 M Lithium Sulfate, 50 % PEG 400, 0.1 M acetate pH 4.0 |