6GX6
Crystal structure of IMP3 RRM12 in complex with RNA (ACAC)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-05-11 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.9999 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 75.440, 75.440, 66.260 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.520 - 2.000 |
R-factor | 0.1834 |
Rwork | 0.180 |
R-free | 0.23590 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6fq1 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.017 |
Data reduction software | MOSFLM (CCP4 7.0.050) |
Data scaling software | SCALA (CCP4 7.0.050) |
Phasing software | PHASER (CCP4 7.0.050) |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 66.260 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.092 | 1.165 |
Number of reflections | 15116 | 2153 |
<I/σ(I)> | 18.2 | 2.4 |
Completeness [%] | 100.0 | 100 |
Redundancy | 12.6 | 12 |
CC(1/2) | 0.999 | 0.600 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293.15 | 0.2M KH2PO4, 20% PEG3350 |