6GWJ
Human OSGEP / LAGE3 / GON7 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-01-25 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.978570 |
Spacegroup name | P 43 |
Unit cell lengths | 105.120, 105.120, 51.350 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.140 - 1.950 |
R-factor | 0.188 |
Rwork | 0.186 |
R-free | 0.21700 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.010 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 46.140 | 46.140 | 2.060 |
High resolution limit [Å] | 1.950 | 5.800 | 1.950 |
Rmerge | 0.066 | 0.033 | 1.097 |
Rmeas | 0.071 | 0.035 | 1.188 |
Number of reflections | 41359 | 1639 | 6542 |
<I/σ(I)> | 15.97 | 49.81 | 1.38 |
Completeness [%] | 99.6 | 99.5 | 98.1 |
Redundancy | 7.308 | 6.969 | 6.862 |
CC(1/2) | 0.999 | 0.999 | 0.585 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | of PEG 4000, 0.1 M Tris HCl pH 8.5 and 0.2 M Magnesium Chloride |