6GWA
Concanavalin B structure determined with data from the EuXFEL, the first MHz free electron laser
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | FREE ELECTRON LASER |
Source details | EUROPEAN XFEL BEAMLINE SPB/SFX |
Synchrotron site | European XFEL |
Beamline | SPB/SFX |
Temperature [K] | 293 |
Detector technology | PIXEL |
Collection date | 2018-06-17 |
Detector | AGIPD |
Wavelength(s) | 1.660 |
Spacegroup name | P 61 |
Unit cell lengths | 82.250, 82.250, 103.400 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 41.841 - 2.100 |
R-factor | 0.1647 |
Rwork | 0.162 |
R-free | 0.21880 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1cnv |
RMSD bond length | 0.009 |
RMSD bond angle | 1.139 |
Data reduction software | CrystFEL |
Data scaling software | CrystFEL |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.000 | 2.200 |
High resolution limit [Å] | 2.100 | 2.100 |
Number of reflections | 23105 | |
<I/σ(I)> | 6.9 | |
Completeness [%] | 100.0 | |
Redundancy | 650 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 293 | Batch mode, acetone |