6GUV
BTB domain of mouse PATZ1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-07-18 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.97625 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 43.232, 43.232, 162.946 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.786 - 2.290 |
R-factor | 0.2112 |
Rwork | 0.209 |
R-free | 0.24480 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1buo |
RMSD bond length | 0.002 |
RMSD bond angle | 0.433 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.230 | 2.370 |
High resolution limit [Å] | 2.290 | 2.290 |
Rmerge | 0.050 | 0.670 |
Rmeas | 0.076 | 0.950 |
Rpim | 0.054 | 0.670 |
Number of reflections | 7573 | 724 |
<I/σ(I)> | 9.91 | 1.39 |
Completeness [%] | 99.6 | 99.18 |
Redundancy | 2 | 2 |
CC(1/2) | 0.998 | 0.551 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 291 | MMT ( DL-Malic acid, MES monohydrate ,Tris) 0.1M PEG 1500, 25% w/v |