6GUU
Structure of CHD5 PHD2 - tandem chromodomains
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-11-23 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97265 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 131.628, 131.628, 84.569 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 51.940 - 2.950 |
R-factor | 0.2091 |
Rwork | 0.206 |
R-free | 0.26300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4o9i |
RMSD bond length | 0.004 |
RMSD bond angle | 0.686 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 51.940 | 3.056 |
High resolution limit [Å] | 2.950 | 2.950 |
Rmerge | 0.025 | 0.541 |
Rmeas | 0.035 | 0.765 |
Number of reflections | 16801 | |
<I/σ(I)> | 17.18 | |
Completeness [%] | 100.0 | |
Redundancy | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 0.2 M ammonium nitrate 20 % PEG 3350 2 % benzamidine hydrochloride |