6GTT
Human STK10 bound to BIRB-796
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-02-20 |
Detector | DECTRIS PILATUS3 R CdTe 300K |
Wavelength(s) | 0.9282 |
Spacegroup name | P 64 2 2 |
Unit cell lengths | 100.667, 100.667, 145.786 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 87.180 - 2.250 |
R-factor | 0.24358 |
Rwork | 0.240 |
R-free | 0.30104 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4use |
RMSD bond length | 0.006 |
RMSD bond angle | 1.111 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0222) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 87.180 | 2.320 |
High resolution limit [Å] | 2.250 | 2.250 |
Rmerge | 0.070 | |
Number of reflections | 21422 | 1920 |
<I/σ(I)> | 22.8 | 2.1 |
Completeness [%] | 100.0 | 100 |
Redundancy | 17.7 | 18.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 277 | 20% PEG6000, 10% ethylene glycol, 0.1M MES pH 6.0, 0.1M magnesium chloride |