6GRS
Paired immunoglobulin-like receptor B (PirB) or Leukocyte immunoglobulin-like receptor subfamily B member 3 (LILRB3) full extracellular domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-08-29 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.0000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 54.690, 185.289, 99.080 |
Unit cell angles | 90.00, 105.56, 90.00 |
Refinement procedure
Resolution | 52.686 - 3.400 |
R-factor | 0.2581 |
Rwork | 0.256 |
R-free | 0.30750 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2d3v 4lla |
RMSD bond length | 0.002 |
RMSD bond angle | 0.604 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 52.690 | 3.630 |
High resolution limit [Å] | 3.400 | 3.400 |
Rmerge | 0.108 | 0.824 |
Number of reflections | 25778 | 4683 |
<I/σ(I)> | 6.9 | 1.8 |
Completeness [%] | 98.8 | 99.2 |
Redundancy | 3.2 | 3.2 |
CC(1/2) | 0.949 | 0.586 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 293.15 | 1.2 M LiCl, 12% PEG 6000m 0.1 M Citric acid buffer pH 5.5 |