6GRQ
Paired immunoglobulin-like receptor B (PirB) or Leukocyte immunoglobulin-like receptor subfamily B member 3 (LILRB3) full extracellular domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-10-23 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 41 2 2 |
Unit cell lengths | 106.375, 106.375, 217.980 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 53.190 | 3.560 |
High resolution limit [Å] | 3.300 | 3.300 |
Rmerge | 0.277 | 2.767 |
Number of reflections | 19634 | 3949 |
<I/σ(I)> | 8.2 | 1.5 |
Completeness [%] | 100.0 | 100 |
Redundancy | 22.3 | 22.5 |
CC(1/2) | 0.998 | 0.542 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 293.15 | 1.1 M LiCL, 14% PEG 6000, 0.1M citic acid buffer pH 5.5 |