6GJ4
Tubulin-6j complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-12-14 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1.00001 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 104.970, 157.810, 181.220 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.022 - 2.400 |
R-factor | 0.199 |
Rwork | 0.197 |
R-free | 0.24060 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 4i4t |
RMSD bond length | 0.003 |
RMSD bond angle | 0.628 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.022 | 2.460 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.146 | 2.499 |
Rmeas | 0.158 | 2.706 |
Rpim | 0.064 | 1.105 |
Number of reflections | 117973 | 8642 |
<I/σ(I)> | 8.7 | 0.8 |
Completeness [%] | 100.0 | 100 |
Redundancy | 6.7 | 6.7 |
CC(1/2) | 0.996 | 0.346 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.7 | 293 | 10% PEG 4K, 12.5% GLYCEROL, 30 MM MAGNESIUM CHLORIDE, 30 MM CALCIUM CHLORIDE, 0.1M MES / 0.1M IMIDAZOLE |