6GIE
Crystal structure of the Acinetobacter baumannii outer membrane protein Omp33
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-10-10 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97834 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 69.680, 73.740, 53.030 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.100 - 2.100 |
R-factor | 0.216 |
Rwork | 0.213 |
R-free | 0.26645 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | previous SAD not deposited |
RMSD bond length | 0.018 |
RMSD bond angle | 1.860 |
Data reduction software | XDS ((1.12_2829: ???)) |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0216) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.100 | 2.200 |
High resolution limit [Å] | 2.100 | 2.100 |
Rpim | 0.048 | 0.630 |
Number of reflections | 16543 | |
<I/σ(I)> | 9.5 | |
Completeness [%] | 100.0 | |
Redundancy | 7.1 | |
CC(1/2) | 0.380 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 26% PEG 400 0.05M NaCl 0.1M sodium citrate pH5.5 |