6GF0
Lysozyme structure determined from SFX data using a Sheet-on-Sheet chipless chip
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | FREE ELECTRON LASER |
Source details | SACLA BEAMLINE BL3 |
Synchrotron site | SACLA |
Beamline | BL3 |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2017-12-18 |
Detector | MPCCD |
Wavelength(s) | 1.770 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 79.100, 79.100, 39.200 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.550 - 2.070 |
R-factor | 0.20034 |
Rwork | 0.199 |
R-free | 0.23483 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 4n5r |
RMSD bond length | 0.006 |
RMSD bond angle | 0.962 |
Data reduction software | CrystFEL |
Data scaling software | CrystFEL |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.200 |
High resolution limit [Å] | 2.070 | 2.070 |
Number of reflections | 7417 | |
<I/σ(I)> | 10.3 | 2.8 |
Completeness [%] | 100.0 | 100 |
Redundancy | 283 | 42 |
CC(1/2) | 0.986 | 0.773 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 293 | 20 % NaCl, 6 % PEG 6000, 0.1 M sodium acetate pH 3.0 |