6GD1
Structure of HuR RRM3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-10-06 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.042 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 42.920, 67.660, 70.140 |
Unit cell angles | 90.00, 91.01, 90.00 |
Refinement procedure
Resolution | 8.980 - 2.010 |
R-factor | 0.17943 |
Rwork | 0.176 |
R-free | 0.24417 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2trx |
RMSD bond length | 0.017 |
RMSD bond angle | 1.819 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0189) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 8.990 | 2.060 |
High resolution limit [Å] | 2.010 | 2.010 |
Rmeas | 0.100 | 0.850 |
Number of reflections | 26790 | 1988 |
<I/σ(I)> | 12.48 | 2.2 |
Completeness [%] | 99.7 | 99.4 |
Redundancy | 6.73 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 23% (w/v) PEG 2000 MME, 0.1 M potassium thiocyanate |