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6GAQ

Crystal structure of oxidised Flavodoxin 2 from Bacillus cereus

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X10SA
Synchrotron siteSLS
BeamlineX10SA
Temperature [K]100
Detector technologyPIXEL
Collection date2012-02-26
DetectorDECTRIS PILATUS 6M
Wavelength(s)0.9999
Spacegroup nameC 2 2 21
Unit cell lengths101.010, 125.451, 59.260
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution62.725 - 2.500
R-factor0.238
Rwork0.235
R-free0.29320
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)6fsg
RMSD bond length0.002
RMSD bond angle0.543
Data reduction softwareMOSFLM
Data scaling softwareAimless
Phasing softwarePHASER
Refinement softwarePHENIX ((1.13_2998: ???))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]62.7302.600
High resolution limit [Å]2.5002.500
Rmerge0.1750.995
Rmeas0.2001.133
Number of reflections133616460
<I/σ(I)>6.41.6
Completeness [%]99.899.9
Redundancy4.14.3
CC(1/2)0.9920.633
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP2980.2 M calcium acetate, 40% (v/v) PEG300 and 0.1M sodium cacodylate pH 6.5

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