6G86
Structure of Cdc14 bound to SIC1 PxL motif
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-09-29 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.28 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 75.090, 94.321, 127.656 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 63.800 - 1.740 |
R-factor | 0.1671 |
Rwork | 0.166 |
R-free | 0.19870 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ohc |
RMSD bond length | 0.010 |
RMSD bond angle | 1.017 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 63.800 | 1.800 |
High resolution limit [Å] | 1.740 | 1.740 |
Rmerge | 0.060 | 0.950 |
Rpim | 0.500 | |
Number of reflections | 93481 | 42727 |
<I/σ(I)> | 11.8 | 1.65 |
Completeness [%] | 99.6 | 98.5 |
Redundancy | 5.1 | 4.7 |
CC(1/2) | 0.999 | 0.520 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 293 | 0.1 M MES pH6, 18% PEG200, 5% PEG 3000 |