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6G78

RSK4 N-terminal Kinase Domain S232E in complex with AMP-PNP

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I24
Synchrotron siteDiamond
BeamlineI24
Temperature [K]100
Detector technologyPIXEL
Collection date2015-10-15
DetectorDECTRIS PILATUS 2M
Wavelength(s)0.979480
Spacegroup nameP 1 21 1
Unit cell lengths52.015, 110.614, 66.559
Unit cell angles90.00, 90.22, 90.00
Refinement procedure
Resolution28.515 - 2.500
R-factor0.2265
Rwork0.226
R-free0.23960
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)6g77
RMSD bond length0.006
RMSD bond angle0.968
Data reduction softwareXDS
Data scaling softwareAimless
Phasing softwarePHASER
Refinement softwarePHENIX (1.9_1692)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]28.5202.589
High resolution limit [Å]2.5002.500
Rmerge0.025
Number of reflections26061857
<I/σ(I)>2.36
Completeness [%]99.899.9
Redundancy3.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP829120 % PEG 6000, 0.1 M TRIS pH8, 2 mM Zinc chloride

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