6G4R
Corynebacterium glutamicum OxyR C206S mutant, H2O2-bound
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-12-14 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 71.216, 56.991, 154.182 |
Unit cell angles | 90.00, 98.02, 90.00 |
Refinement procedure
Resolution | 76.340 - 2.620 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.32) |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 153.000 | 153.000 | 2.690 |
High resolution limit [Å] | 2.620 | 11.720 | 2.620 |
Rmerge | 0.246 | 0.103 | 2.039 |
Rmeas | 0.268 | 0.113 | 2.217 |
Rpim | 0.105 | 0.046 | 0.861 |
Total number of observations | 241902 | 2759 | 17931 |
Number of reflections | 37454 | 463 | 2762 |
<I/σ(I)> | 5.3 | 12.7 | 1.4 |
Completeness [%] | 100.0 | 99.9 | 100 |
Redundancy | 6.5 | 6 | 6.5 |
CC(1/2) | 0.987 | 0.983 | 0.336 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.2 | 283 | PEG 4000, 2-(N-morpholino)ethanesulfonic acid (MES), lithium sulfate, TCEP |