6G4D
Crystal structure of the omega TRANSAMINASE FROM PSEUDOMONAS Jessenii in complex with PLP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR-H |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 2015-10-06 |
Detector | MARRESEARCH |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 |
Unit cell lengths | 98.810, 98.810, 119.160 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.600 - 2.150 |
R-factor | 0.229 |
Rwork | 0.227 |
R-free | 0.26100 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | D_1200009303 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.324 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.600 | 2.210 |
High resolution limit [Å] | 2.150 | 2.150 |
Rpim | 0.052 | 0.351 |
Number of reflections | 62118 | |
<I/σ(I)> | 45 | 2.1 |
Completeness [%] | 100.0 | 100 |
Redundancy | 4.4 | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 294 | 1.0 M Sodium succinate pH 7.5 |