6G4C
Crystal structure of the omega transaminase from Pseudomonas jessenii in the apo form, crystallized from ammonium phosphate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR-H |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 2015-04-09 |
Detector | MARRESEARCH |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 |
Unit cell lengths | 98.296, 98.296, 119.924 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 51.200 - 1.870 |
R-factor | 0.1691 |
Rwork | 0.168 |
R-free | 0.19207 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | D_1200009303 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.398 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 51.200 | 1.900 |
High resolution limit [Å] | 1.870 | 1.870 |
Rpim | 0.034 | 0.357 |
Number of reflections | 94352 | 4457 |
<I/σ(I)> | 19.9 | 2.1 |
Completeness [%] | 99.7 | 94.9 |
Redundancy | 4.1 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 294 | 1.0 M ammonium phosphate |