6G4B
Crystal structure of the omega transaminase from Pseudomonas jessenii in the apo form, crystallized from succinate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 2015-03-11 |
Detector | MARRESEARCH |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 |
Unit cell lengths | 98.240, 98.240, 119.050 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.900 - 1.800 |
R-factor | 0.1418 |
Rwork | 0.141 |
R-free | 0.16575 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4grx |
RMSD bond length | 0.009 |
RMSD bond angle | 1.345 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.900 | 1.830 |
High resolution limit [Å] | 1.800 | 1.800 |
Rpim | 0.038 | 0.402 |
Number of reflections | 104659 | 4975 |
<I/σ(I)> | 17 | 2 |
Completeness [%] | 99.8 | 95.3 |
Redundancy | 7.4 | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 294 | 1.0 M Sodium succinate, pH 7.5 |