6G3J
MHC A02 Allele presenting MTSAIGILVP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-01-26 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.96859 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 202.940, 50.280, 119.070 |
Unit cell angles | 90.00, 122.86, 90.00 |
Refinement procedure
Resolution | 41.050 - 2.450 |
R-factor | 0.22569 |
Rwork | 0.223 |
R-free | 0.27021 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5eu5 |
RMSD bond length | 0.018 |
RMSD bond angle | 1.900 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0189) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.050 | 2.510 |
High resolution limit [Å] | 2.450 | 2.450 |
Rmerge | 0.104 | 1.155 |
Rmeas | 0.123 | 1.354 |
Number of reflections | 37034 | 2764 |
<I/σ(I)> | 9.1 | 1 |
Completeness [%] | 98.7 | 97.5 |
Redundancy | 3.5 | 3.6 |
CC(1/2) | 0.993 | 0.594 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 |