6G2K
Structure of HuR RRM3 in complex with RNA (UUUUUU)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-04-19 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 34.310, 79.740, 51.070 |
Unit cell angles | 90.00, 93.14, 90.00 |
Refinement procedure
Resolution | 8.980 - 2.010 |
R-factor | 0.1719 |
Rwork | 0.169 |
R-free | 0.23489 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.017 |
RMSD bond angle | 1.767 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0189) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 8.990 | 2.060 |
High resolution limit [Å] | 2.010 | 2.010 |
Rmeas | 0.137 | 0.965 |
Number of reflections | 18274 | |
<I/σ(I)> | 13.4 | |
Completeness [%] | 99.7 | |
Redundancy | 6.82 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M TRIS pH 8.5 and 2.25 M ammonium sulphate |