6G2C
X-ray structure of NSD3-PWWP1 in complex with compound 9
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-12-09 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1.000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.911, 47.570, 64.287 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.240 - 1.760 |
R-factor | 0.203 |
Rwork | 0.201 |
R-free | 0.23000 |
RMSD bond length | 0.008 |
RMSD bond angle | 0.870 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.17) |
Phasing software | BALBES |
Refinement software | BUSTER (2.11.7) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.240 | 1.763 |
High resolution limit [Å] | 1.757 | 1.757 |
Rmeas | 0.074 | 0.861 |
Rpim | 0.029 | 0.337 |
Number of reflections | 12491 | 1996 |
<I/σ(I)> | 16.5 | 2.3 |
Completeness [%] | 89.6 | 96.1 |
Redundancy | 6.3 | 6.2 |
CC(1/2) | 0.999 | 0.788 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 277 | 100mM Morpheus Buffer 3, 30% P550MME_P20K, 10% Morpheus Ethylene glycols |