6FYU
Structure of H7(A/Shanghai/2/2013) Influenza Hemagglutinin in complex SD36
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-B |
Synchrotron site | APS |
Beamline | 23-ID-B |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-10-24 |
Detector | MARRESEARCH |
Wavelength(s) | 1.0332 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 101.424, 128.159, 192.104 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.026 - 2.643 |
R-factor | 0.1872 |
Rwork | 0.186 |
R-free | 0.21620 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.731 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (dev_1839) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.740 |
High resolution limit [Å] | 2.640 | 2.640 |
Rpim | 0.050 | |
Number of reflections | 73520 | |
<I/σ(I)> | 13.2 | |
Completeness [%] | 100.0 | |
Redundancy | 7.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.2 M Tri-potassium citrate, 20 % PEG3350 |