6FXO
Crystal structure of Major Bifunctional Autolysin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-10-05 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.918400 |
Spacegroup name | P 64 2 2 |
Unit cell lengths | 110.168, 110.168, 92.390 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 35.400 - 2.500 |
R-factor | 0.2948 |
Rwork | 0.295 |
R-free | 0.33000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | SagB |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | MAIN |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.390 | 2.410 |
High resolution limit [Å] | 2.280 | 2.280 |
Rmeas | 0.091 | 1.626 |
Number of reflections | 15697 | 2453 |
<I/σ(I)> | 25.31 | 1.96 |
Completeness [%] | 99.8 | 99.3 |
Redundancy | 21.1 | |
CC(1/2) | 1.000 | 0.631 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 2 M Ammonium sulphate |