6FV7
Dimer structure of the MATE family multidrug resistance transporter Aq_128 from Aquifex aeolicus in the outward-facing state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-12-04 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 72.600, 116.500, 142.600 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.884 - 3.700 |
R-factor | 0.3288 |
Rwork | 0.327 |
R-free | 0.35920 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6fv6 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.538 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 3.830 |
High resolution limit [Å] | 3.700 | 3.700 |
Rmerge | 0.233 | 1.109 |
Rmeas | 0.257 | |
Rpim | 0.107 | 0.482 |
Number of reflections | 13317 | 1314 |
<I/σ(I)> | 5 | 1.5 |
Completeness [%] | 99.7 | 99.8 |
Redundancy | 5.7 | 6 |
CC(1/2) | 0.996 | 0.790 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 6 | 295 | 0.1 M Sodium chloride 0.1 M Magnesium chloride 0.1 M MES 40 % PEG 200 (v/v) |