6FS0
INDUCED MYELOID LEUKEMIA CELL DIFFERENTIATION PROTEIN FABCOMPLEX IN COMPLEX WITH AZD5991
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-04-10 |
Detector | DECTRIS PILATUS3 X 1M |
Wavelength(s) | 0.97858 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 147.200, 42.050, 107.290 |
Unit cell angles | 90.00, 113.17, 90.00 |
Refinement procedure
Resolution | 28.150 - 2.250 |
R-factor | 0.195 |
Rwork | 0.193 |
R-free | 0.23300 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.150 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.6) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.320 | 2.320 |
High resolution limit [Å] | 2.240 | 2.240 |
Number of reflections | 29214 | |
<I/σ(I)> | 9 | |
Completeness [%] | 99.4 | |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 293 | 0.1M sodium acetate-HCL pH 4.6 18%W/V PEG-8000 0.2M calcium acetate |