6FRH
Crystal structure of Ssp DnaB Mini-Intein variant M86
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-08-11 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.9793 |
Spacegroup name | P 1 |
Unit cell lengths | 34.635, 40.941, 57.906 |
Unit cell angles | 84.37, 83.45, 65.00 |
Refinement procedure
Resolution | 31.951 - 2.030 |
R-factor | 0.2228 |
Rwork | 0.222 |
R-free | 0.24170 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1mi8 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.492 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.32) |
Phasing software | PHASER |
Refinement software | PHENIX (dev_2733) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 37.050 | 37.050 | 2.080 |
High resolution limit [Å] | 2.030 | 9.060 | 2.030 |
Rmerge | 0.154 | 0.086 | 0.757 |
Rmeas | 0.183 | 0.101 | 0.897 |
Rpim | 0.098 | 0.052 | 0.475 |
Number of reflections | 18028 | 205 | 1329 |
<I/σ(I)> | 5.8 | ||
Completeness [%] | 96.8 | 98.1 | 96.2 |
Redundancy | 3.4 | 3.6 | 3.5 |
CC(1/2) | 0.982 | 0.991 | 0.706 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.6 | 293 | 0.1 M Tris pH 7.6, 22 % PEG4000 |