6FPB
Crystal structure of anti-mTFP1 DARPin 1238_G01 in space group I4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-11-19 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.99986 |
Spacegroup name | I 4 |
Unit cell lengths | 66.224, 66.224, 77.913 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.827 - 1.617 |
R-factor | 0.1526 |
Rwork | 0.151 |
R-free | 0.17460 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ydy |
RMSD bond length | 0.009 |
RMSD bond angle | 1.017 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10pre_2131: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.827 | 1.720 |
High resolution limit [Å] | 1.617 | 1.617 |
Rmeas | 0.066 | 0.935 |
Number of reflections | 41912 | 4096 |
<I/σ(I)> | 11.5 | 1.3 |
Completeness [%] | 99.3 | 97.1 |
Redundancy | 2.2 | 2.2 |
CC(1/2) | 0.998 | 0.746 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 293 | 2 M NaCl, 10% PEG10000 |