6FOM
Copper transporter OprC
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-08-07 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9159 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 62.129, 170.556, 197.374 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.260 - 2.900 |
R-factor | 0.217 |
Rwork | 0.214 |
R-free | 0.27000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6fok |
RMSD bond length | 0.009 |
RMSD bond angle | 1.290 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.260 | 3.010 |
High resolution limit [Å] | 2.900 | 2.900 |
Number of reflections | 42339 | 0 |
<I/σ(I)> | 7 | |
Completeness [%] | 89.1 | |
Redundancy | 5.5 | |
CC(1/2) | 0.990 | 0.500 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.1 M sodium chloride 0.15 M ammonium sulfate 0.01 M MES sodium 19% (w/v) PEG1000 |