6FOK
Copper transporter OprC
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-10-08 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.3785 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 156.370, 196.720, 166.350 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 84.670 - 1.970 |
R-factor | 0.211 |
Rwork | 0.210 |
R-free | 0.23200 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 0.925 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 84.670 | 2.020 |
High resolution limit [Å] | 1.970 | 1.970 |
Number of reflections | 178934 | 0 |
<I/σ(I)> | 15.8 | |
Completeness [%] | 99.5 | |
Redundancy | 25.4 | |
CC(1/2) | 0.990 | 0.500 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.1 M NaCl 0.15 M NH4SO4 0.1 M MES 18-22% PEG1000 3 mM CuCl2 |