6FMX
IMISX-EP of W-PgpB
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-07-01 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1.21371 |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 68.757, 76.801, 98.912 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 35.614 - 1.790 |
| R-factor | 0.2379 |
| Rwork | 0.237 |
| R-free | 0.26240 |
| Structure solution method | SAD |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.822 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | SHELXCD |
| Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 35.614 | 1.900 |
| High resolution limit [Å] | 1.790 | 1.790 |
| Rmeas | 0.100 | 1.320 |
| Number of reflections | 39988 | 6925 |
| <I/σ(I)> | 7.93 | 0.91 |
| Completeness [%] | 91.7 | 90 |
| Redundancy | 2.6 | 2.5 |
| CC(1/2) | 0.920 | 0.500 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | LIPIDIC CUBIC PHASE | 293 | 40 %(v/v) PEG-400, 100 mM HEPES pH 7 and 100 mM lithium citrate tribasic tetrahydrate |
