6FMV
IMISX-EP of Hg-BacA soaking SIRAS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-10-23 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.9 |
Spacegroup name | C 2 2 2 |
Unit cell lengths | 113.390, 144.370, 40.390 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.390 - 2.300 |
R-factor | 0.1954 |
Rwork | 0.194 |
R-free | 0.22240 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELXCD |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.390 | 2.360 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmeas | 0.500 | 6.390 |
Number of reflections | 15224 | 2127 |
<I/σ(I)> | 9.85 | |
Completeness [%] | 100.0 | 100 |
Redundancy | 16.95 | 14.09 |
CC(1/2) | 0.990 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 293 | 40 % PEG-400, 0.3-0.5 M ammonium citrate dibasic and 0.1 M sodium citrate pH 5.0 |