6FM0
Deoxyguanylosuccinate synthase (DgsS) and ATP structure at 1.7 Angstrom resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-10-09 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.978570 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 158.860, 60.410, 91.030 |
Unit cell angles | 90.00, 114.76, 90.00 |
Refinement procedure
Resolution | 45.600 - 1.700 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.600 | 1.800 |
High resolution limit [Å] | 1.700 | 1.700 |
Number of reflections | 884293 | |
<I/σ(I)> | 11.65 | |
Completeness [%] | 97.1 | |
Redundancy | 4.99 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 20% PEG3350 0.2M Na2SO4 |