6FLJ
Crystal structure of Cep120 C2A_K76A mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-05-17 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.842, 51.367, 66.757 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.710 - 1.751 |
R-factor | 0.2117 |
Rwork | 0.210 |
R-free | 0.24570 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4icw |
RMSD bond length | 0.012 |
RMSD bond angle | 1.243 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((dev_2863: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.710 | 1.814 |
High resolution limit [Å] | 1.750 | 1.751 |
Rmerge | 0.069 | 1.925 |
Rmeas | 0.072 | |
Rpim | 0.020 | 0.567 |
Number of reflections | 14678 | 1425 |
<I/σ(I)> | 24.44 | 1.29 |
Completeness [%] | 99.9 | 99.65 |
Redundancy | 12.7 | 12.2 |
CC(1/2) | 1.000 | 0.712 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 20% PEG 3350 and 0.2 M NaSCN |