6FLF
Deoxyguanylosuccinate synthase (DgsS) structure at 1.33 Angstrom resolution.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-10-09 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.978570 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 90.920, 59.480, 73.980 |
Unit cell angles | 90.00, 102.67, 90.00 |
Refinement procedure
Resolution | 49.400 - 1.330 |
R-factor | 0.201 |
Rwork | 0.200 |
R-free | 0.22600 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.040 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.400 | 1.410 |
High resolution limit [Å] | 1.330 | 1.330 |
Number of reflections | 88372 | |
<I/σ(I)> | 8.4 | |
Completeness [%] | 99.2 | |
Redundancy | 4.74 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 2M NaCl 12% PEG 6K |