6FLC

2C8 Fab bound to EDIII of DenV 2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-2
Synchrotron site	ESRF
Beamline	ID14-2
Temperature [K]	100
Detector technology	CCD
Collection date	2008-07-20
Detector	ADSC QUANTUM 315
Wavelength(s)	0.98
Spacegroup name	P 1
Unit cell lengths	42.560, 61.416, 104.594
Unit cell angles	77.54, 81.11, 85.53

Refinement procedure

Resolution	33.700 - 2.000
R-factor	0.1817
Rwork	0.180
R-free	0.21600
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	1.130
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	MOLREP
Refinement software	BUSTER (2.9.2)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	33.700	2.100
High resolution limit [Å]	2.000	2.000
Number of reflections	66849
<I/σ(I)>	15
Completeness [%]	97.0
Redundancy	3.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		294	Read the paper