6FHQ
Crystal structure of human BAZ2B PHD zinc finger in complex with Fr 21
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-30 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9686 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 38.339, 45.369, 65.039 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.240 - 1.950 |
R-factor | 0.1872 |
Rwork | 0.185 |
R-free | 0.23884 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 4qf3 |
RMSD bond length | 0.020 |
RMSD bond angle | 1.880 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 65.040 | 2.000 |
High resolution limit [Å] | 1.950 | 1.950 |
Rmerge | 0.081 | |
Number of reflections | 8453 | 527 |
<I/σ(I)> | 11.4 | |
Completeness [%] | 97.7 | |
Redundancy | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 291 | 2.2 - 2.4 M sodium/ potassium phosphate |