6FH4
CtsR C-terminal domain with bound phospho-arginine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2016-02-01 |
Detector | MARRESEARCH |
Wavelength(s) | 1.542 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 44.100, 135.550, 59.120 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.899 - 2.490 |
R-factor | 0.2475 |
Rwork | 0.244 |
R-free | 0.27660 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3h0d |
RMSD bond length | 0.007 |
RMSD bond angle | 1.192 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13rc1_2961: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.899 | 2.579 |
High resolution limit [Å] | 2.490 | 2.490 |
Number of reflections | 13014 | |
<I/σ(I)> | 5.73 | |
Completeness [%] | 99.8 | |
Redundancy | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.25 | 292.15 | 10% v/v polypropylene glycol P 400 |