6FGZ
Cyanidioschyzon merolae Dnm1 (CmDnm1)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 80 |
Detector technology | CCD |
Collection date | 2006-06-01 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.9330 |
Spacegroup name | P 62 2 2 |
Unit cell lengths | 188.219, 188.219, 163.627 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.838 - 7.002 |
R-factor | 0.3507 |
Rwork | 0.344 |
R-free | 0.41120 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4bej |
RMSD bond length | 0.022 |
RMSD bond angle | 2.135 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (dev_1932) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.838 | 7.380 |
High resolution limit [Å] | 7.000 | 7.000 |
Rmerge | 0.140 | |
Number of reflections | 2963 | |
<I/σ(I)> | 19.5 | |
Completeness [%] | 99.5 | |
Redundancy | 18.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 1.0 M ammonium phosphate, 0.1 M lithium sulphate and 0.1 M sodium acetate pH 4.6 |