6FGD
Crystal structure of Gephyrin E domain in complex with Artemether
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-04-24 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9762 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 87.152, 99.455, 111.965 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.580 - 1.500 |
R-factor | 0.15 |
Rwork | 0.149 |
R-free | 0.17800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5err |
RMSD bond length | 0.008 |
RMSD bond angle | 1.077 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11_2567: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.580 | 1.530 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.081 | 1.284 |
Rmeas | 0.096 | 1.527 |
Rpim | 0.051 | 0.816 |
Number of reflections | 77361 | |
<I/σ(I)> | 11.2 | |
Completeness [%] | 99.5 | |
Redundancy | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 293 | 0.1 M sodium acetate 20-36% MPD |