6FF2
CopZ metallochaperone
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-11-25 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 26.619, 49.460, 102.829 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 51.410 - 1.300 |
R-factor | 0.16655 |
Rwork | 0.165 |
R-free | 0.20194 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2qif |
RMSD bond length | 0.017 |
RMSD bond angle | 1.745 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 51.410 | 1.320 |
High resolution limit [Å] | 1.300 | 1.300 |
Number of reflections | 34140 | 1649 |
<I/σ(I)> | 10.5 | 1.6 |
Completeness [%] | 99.6 | 99.4 |
Redundancy | 4.6 | 4.8 |
CC(1/2) | 0.999 | 0.462 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 200 mM MgCl2, 100 mM HEPES pH 7.0, 20%w/v PEG 6000 |