6FDO

Rio2 structure

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 1
Synchrotron site	SOLEIL
Beamline	PROXIMA 1
Temperature [K]	110
Detector technology	CCD
Collection date	2010-09-01
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.9789
Spacegroup name	P 65
Unit cell lengths	67.555, 67.555, 312.195
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	42.690 - 2.600
R-factor	0.198
Rwork	0.195
R-free	0.25000
Structure solution method	FOURIER SYNTHESIS
RMSD bond length	0.010
RMSD bond angle	1.200
Data reduction software	XDS
Data scaling software	XDS
Refinement software	BUSTER (2.10.3)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	42.690	2.690
High resolution limit [Å]	2.600	2.600
Rpim	0.058	0.732
Number of reflections	279056	31169
<I/σ(I)>	8.73	1.49
Completeness [%]	100.0	100
Redundancy	11.3	12.9
CC(1/2)	0.991	0.493

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		298	Morpheus D2