6FDO
Rio2 structure
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SOLEIL BEAMLINE PROXIMA 1 |
| Synchrotron site | SOLEIL |
| Beamline | PROXIMA 1 |
| Temperature [K] | 110 |
| Detector technology | CCD |
| Collection date | 2010-09-01 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9789 |
| Spacegroup name | P 65 |
| Unit cell lengths | 67.555, 67.555, 312.195 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 42.690 - 2.600 |
| R-factor | 0.198 |
| Rwork | 0.195 |
| R-free | 0.25000 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.200 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Refinement software | BUSTER (2.10.3) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 42.690 | 2.690 |
| High resolution limit [Å] | 2.600 | 2.600 |
| Rpim | 0.058 | 0.732 |
| Number of reflections | 279056 | 31169 |
| <I/σ(I)> | 8.73 | 1.49 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 11.3 | 12.9 |
| CC(1/2) | 0.991 | 0.493 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 298 | Morpheus D2 |
