6FDD
Crystal Structure of the HHD2 Domain of Whirlin
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SOLEIL BEAMLINE PROXIMA 1 |
| Synchrotron site | SOLEIL |
| Beamline | PROXIMA 1 |
| Temperature [K] | 110 |
| Detector technology | PIXEL |
| Collection date | 2016-09-06 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.97917 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 118.580, 74.910, 63.840 |
| Unit cell angles | 90.00, 106.38, 90.00 |
Refinement procedure
| Resolution | 47.610 - 1.750 |
| R-factor | 0.188 |
| Rwork | 0.187 |
| R-free | 0.21000 |
| Structure solution method | SAD |
| RMSD bond length | 0.010 |
| RMSD bond angle | 0.830 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.10.3) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.170 | 1.780 |
| High resolution limit [Å] | 1.750 | 1.750 |
| Rmerge | 0.069 | 0.910 |
| Rpim | 0.047 | 0.630 |
| Number of reflections | 54049 | 2966 |
| <I/σ(I)> | 13 | 1.8 |
| Completeness [%] | 99.9 | 99.9 |
| Redundancy | 5.5 | 5.7 |
| CC(1/2) | 0.997 | 0.681 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 291 | ammonium sulfate 1.26M cacodylate 0.7M |
