6FAP
Crystal structure of human BAZ2A PHD zinc finger in complex with Fr23
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-30 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9686 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 72.796, 72.796, 99.630 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.730 - 2.700 |
R-factor | 0.21078 |
Rwork | 0.209 |
R-free | 0.24798 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4qf2 |
RMSD bond length | 0.005 |
RMSD bond angle | 0.746 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.730 | 2.830 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.148 | 0.680 |
Number of reflections | 7841 | 995 |
<I/σ(I)> | 10.7 | 3.7 |
Completeness [%] | 100.0 | 100 |
Redundancy | 12 | 12.3 |
CC(1/2) | 0.990 | 0.950 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 291 | 2.4 M sodium/ potassium phosphate |