6F9Y
Lysozyme crystallized in presence of 10 mM lithium sulphate at pH 4.5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-07-01 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97926 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 30.131, 56.403, 73.429 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.825 - 1.200 |
R-factor | 0.1688 |
Rwork | 0.167 |
R-free | 0.20090 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4e3u |
RMSD bond length | 0.007 |
RMSD bond angle | 0.908 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.32) |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 19.830 | 19.830 | 1.220 |
High resolution limit [Å] | 1.200 | 6.570 | 1.200 |
Rmerge | 0.072 | 0.060 | 0.589 |
Rmeas | 0.078 | 0.065 | 0.649 |
Rpim | 0.029 | 0.022 | 0.262 |
Total number of observations | 175488 | ||
Number of reflections | 32486 | 206 | 1787 |
<I/σ(I)> | 10.4 | ||
Completeness [%] | 82.3 | 72.6 | 92.9 |
Redundancy | 5.4 | 6.2 | 5.3 |
CC(1/2) | 0.997 | 0.997 | 0.691 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 298 | 10 mM Lithium Sulphate, 0.3 M Sodium Chloride, 0.1 M Sodium Acetate |