6F8P
Crystal structure of Gn from Rift Valley fever virus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-04-26 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97625 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 37.390, 94.180, 97.990 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.990 - 1.600 |
R-factor | 0.1667 |
Rwork | 0.165 |
R-free | 0.19890 |
Structure solution method | SAD |
RMSD bond length | 0.017 |
RMSD bond angle | 1.525 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | autoSHARP |
Refinement software | PHENIX (dev_2283) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.995 | 1.640 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.086 | 1.044 |
Number of reflections | 46607 | 3369 |
<I/σ(I)> | 12.35 | |
Completeness [%] | 99.9 | 99.6 |
Redundancy | 9.7 | 9.47 |
CC(1/2) | 0.998 | 0.818 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 298 | 20% w/v PEG 6000, 0.1 M HEPES pH 7.0 |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 298 | 20% w/v PEG 6000, 0.1 M HEPES pH 7.0 |