Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X9A |
| Synchrotron site | NSLS |
| Beamline | X9A |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2014-06-11 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1.000 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 47.322, 77.000, 137.258 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 68.600 - 2.450 |
| R-factor | 0.2729 |
| Rwork | 0.271 |
| R-free | 0.30490 |
| Structure solution method | SAD |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.334 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 68.600 | 2.490 |
| High resolution limit [Å] | 2.450 | 2.450 |
| Rmerge | 0.094 | 1.120 |
| Number of reflections | 19008 | 962 |
| <I/σ(I)> | 11.2 | 2.2 |
| Completeness [%] | 99.8 | 99.2 |
| Redundancy | 8.7 | 8.7 |
| CC(1/2) | 0.998 | 0.992 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7.3 | 291 | 50 mM Tris pH 7.3 and 40% MPD |
